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K Sections => K1/8 - DC/Low Frequency => Topic started by: Hawaii596 on 10-09-2013 -- 16:58:40

Title: An ISO17025 Question About Derivative Measurements from CMC
Post by: Hawaii596 on 10-09-2013 -- 16:58:40
Okay, Lets say I am accredited to generate (Fluke 5720A) and measure (Fluke 8508A) (for example) 1000 VDC and to measure current (Keithley 263) to as low as about 1 pA (picoamp). But, for example, I am accredited on my CMC to measure up to 2 Giga Ohms.

But, even though I am accredited to 2 Giga Ohms, I can source 1000 ACCREDITED DC Volts across an unknown resistance, and measure the ACCREDITED DC current to as low as 1 picoamp. This combination theoretically results in 10E15 Ohms (1 Peta Ohm = 1,000 Tera Ohms = 1 Million Giga Ohms). There are of course all of the uncertainty contributors of repeatability, drift, resolution, uncertainties of calibrations, etc.  I know how to deal with them.

So although the cumulative uncertainty of a given established resistance would have lots of contributions, would it nevertheless be accreditable? This would be as a derivative measurement to my CMC? Or even if I am able to make the measurement and subsequent derived (possibly) accredited resistance value, would I be limited to CMC, even though my CMC allows me to directly accredit the input parameters (i.e.: voltage source and current measurement).

I could then (if this is accreditable) accredit these values, and make accredited measurements with them which would not exceed my CMC. Or is this the sort of question I should ask my accrediting body?

This seems logically that if I am accredited for the volts source and current measurement to make a resistance measurement that way, that I should be able to RSS together the factors along with the usual suspect contributors to uncertainty, and derive an accredited resistance value (in this case, a Penn Airborne).  And by the way, does anyone know the max voltage specs on the Penn Airborne resistors?  I have had poor luck trying to find them.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Bryan on 10-09-2013 -- 17:05:41
I am curious about that myself, my thoughts are where international agencies are involved creativity & innovation are not welcomed.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: RFCAL on 10-09-2013 -- 17:24:21
To stay out of trouble, you should need to ask your accrediting body for guidance. Remember, you are accredited to 1000V with your 5720A and 1pA with the Keithley 263, but that probably does not equate to being accredited with the Math. That's why you play it safe and get your accreditating body involved.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: USMC kalibrater on 10-10-2013 -- 05:23:14
You can absolutely do this.  You should state how the value was derived(which is redundant being that measuring resistance with a meter is doing basically the same thing), you obviously need to combine uncertainties and there is some additional error to consider.
If you think about Ohms is a derived SI unit anyhow so the math portion is inherent.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Bryan on 10-10-2013 -- 11:32:45
I'd think if the result was tagged as calculated or derived from some recognized formula you'd be in good ethical standing, just my personal opinion
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Hawaii596 on 10-10-2013 -- 12:02:43
I had a meeting with our quality manager this morning and the position for the moment is that we need to ask our accreditation body for their blessing.  I am with you, as I believe it will probably be alright.  But that's the temporary verdict.  If I get a firm answer, I'll post it.  I think that's correct also.  But it would be nice to have an official position on it.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: USMC kalibrater on 10-10-2013 -- 13:08:17
If an AB told me no on this I would challenge it.  If you were trying to calculate a base SI unit then I would say you are questionable but you are calulating a derived SI unit using a perfectly acceptable method. 
Get approval to save hassles later but no way would I concede to a no response.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Hawaii596 on 10-10-2013 -- 15:11:33
The AB responded that Yes, we can make the measurements as outlined.  They reminded us to keep in mind that you cannot report a measurement uncertainty better (lower) on our calibration certificate than the CMC on your scope for Resistance; and, the internal calibrations we perform are subject to witnessing during future assessment.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: CalibratorJ on 10-11-2013 -- 07:14:23
Quote from: Hawaii596 on 10-10-2013 -- 15:11:33
The AB responded that Yes, we can make the measurements as outlined.  They reminded us to keep in mind that you cannot report a measurement uncertainty better (lower) on our calibration certificate than the CMC on your scope for Resistance; and, the internal calibrations we perform are subject to witnessing during future assessment.

So you can measure and accredit higher resistance values than you are scoped for? That's what I am interpreting this to mean. Or am I off?
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Hawaii596 on 10-11-2013 -- 09:37:19
This is why I brought it up with the AB.  The ambiguity is that if we are scoped for sourcing voltage and measuring current that mathematically equates to a resistance, so long as we properly document and account, that it is within our scope.  Our scope is for direct measurement of resistance up to 2 Giga ohms on the Fluke 8508A.  We are (according to the almost verbatim language I posted from the AB in my previous posting) accredited to source the voltage, measure the current and mathematically compute the resistance thereby measured.  So it is higher than what we are scoped to directly measure on our Fluke 8508A, but it is not higher than we are scoped for when measuring resistance by sourcing an accredited voltage and measuring the current (the exact same way the multimeter does it for you).  All the resistance function is on a multimeter is a machine automatically doing the math for you by sourcing a current and measuring a voltage.  The only difference theoretically in many high resistance meters is that they use a capacitive time constant method versus a voltage/current method.  So it is not higher than we are scoped for.  Again, because it is a little ambiguous, and requires understanding the theory of how resistance measurements are made, that also means that I felt the need to make sure the AB was in agreement before proceeding.

This is only strictly under circumstances where we are scoped for both the voltage and current involved in the measurement, that we account for all uncertainties properly, that it does not exceed our scoped CMC for either the voltage or current.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: CalibratorJ on 10-13-2013 -- 08:01:01
Cool. I understand the theory behind the measurements. Just thought it was interesting that any AB would let you and actually tell you that you could accredit values that aren't specifically listed on your scope, derived or not. Make sure you have it in writing from your AB for audit time.

(I would go on a rant about ABs, but I will refrain, don't want to derail the train!)
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: RFCAL on 10-13-2013 -- 12:00:11
Ok, I'll start! Different AB's will let you do anything to collect your$$. That is a fact!! As in cars, there are different models and makes. Depends if you want to drive a Ford or a Caddilac. Same for AB's. Some will tell you you can do whatever it is that you want to do, others will say no,not correct. Remember, you only have to satisfy the AB that accredits you.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Hawaii596 on 10-14-2013 -- 08:33:55
I'll stay out of the fray on this one.  I'm just trying to make sure and understand what is right.  Sounds like this is not a definitive already settled issue.  Guess I will have to read some more as well.  And good tip - my quality manager said about the same thing - to keep their response on file.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: USMC kalibrater on 10-14-2013 -- 10:08:40
Quote from: CalibratorJ on 10-11-2013 -- 07:14:23
Quote from: Hawaii596 on 10-10-2013 -- 15:11:33
The AB responded that Yes, we can make the measurements as outlined.  They reminded us to keep in mind that you cannot report a measurement uncertainty better (lower) on our calibration certificate than the CMC on your scope for Resistance; and, the internal calibrations we perform are subject to witnessing during future assessment.

So you can measure and accredit higher resistance values than you are scoped for? That's what I am interpreting this to mean. Or am I off?

No, thats incorrect.  They are making, voltage and current measurements that they are accredited to do.  Then calculating the resistance.  Same way every other resistance measurement is made except instead of a ohmmeter doing the math, they are

Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: scottbp on 10-15-2013 -- 16:28:36
Okay, I got hammered on an audit for this: We did an accredited calibration for a customer on a power meter that measures watts at 60 Hz (not a watt-hour meter, just a direct reading watt meter). We used a Fluke 5500A to source voltage to the voltage input terminals, and current to the current input terminals. Our AB auditor said we were not supposed to give out an accredited calibration to the customer because we did not have power listed on our scope. I tried to explain that we have voltage and current listed on our scope, and we were mathematically calculating the power and the uncertainty of the voltage and current from the calibrator was well within our scope, and the combined uncertainty was well below the tolerance of the watt meter, but the auditor would not take that as an answer. So now I have to compile an uncertainty budget for power and submit it to the AB to get power put on our scope of accreditation.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: USMC kalibrater on 10-16-2013 -- 03:40:27
Quote from: scottbp on 10-15-2013 -- 16:28:36
Okay, I got hammered on an audit for this: We did an accredited calibration for a customer on a power meter that measures watts at 60 Hz (not a watt-hour meter, just a direct reading watt meter). We used a Fluke 5500A to source voltage to the voltage input terminals, and current to the current input terminals. Our AB auditor said we were not supposed to give out an accredited calibration to the customer because we did not have power listed on our scope. I tried to explain that we have voltage and current listed on our scope, and we were mathematically calculating the power and the uncertainty of the voltage and current from the calibrator was well within our scope, and the combined uncertainty was well below the tolerance of the watt meter, but the auditor would not take that as an answer. So now I have to compile an uncertainty budget for power and submit it to the AB to get power put on our scope of accreditation.
Scott,
So lets break this into a few pieces.
1) They had resistance on their scope already, which tells the auditor they have been proficeincy tested to make resistance measurements and that they understand the measurement.
2) They are not directly measuring the resistor they are measuring values they are accredited to measure.
Do you have a voltmeter and ammeter in circuit? Using a 5500 to cal a watt meter  means to me that you have a direct connection to the Wattmeter and in such a case you are not measuring Volts and current and calculating power.

The biggest difference is that they have resistance listed on their scope already. 
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: flew-da-coup on 10-16-2013 -- 08:01:37
Quote from: USMC kalibrater on 10-10-2013 -- 05:23:14
You can absolutely do this.  You should state how the value was derived(which is redundant being that measuring resistance with a meter is doing basically the same thing), you obviously need to combine uncertainties and there is some additional error to consider.

I completely agree. This should be a non-issue.
If you think about Ohms is a derived SI unit anyhow so the math portion is inherent.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: Hawaii596 on 10-16-2013 -- 12:08:34
Let me re-iterate that I don't want to be the one who stirs the pot here.  I am the one seeking truth.  So I honestly feel your pain, ScottBP.  And I will certainly be taking those details into account.  So again, as the learner here, I'm wondering if on the certificate where a value was certified as what I'm calling a "Derivative" value, I wonder if (as in my case), if I stated the two accredited measurements as those accredited in my scope, included their expanded uncertainties, then stated the other was a derived value, stated the combined RSS calculated expanded uncertainty, would the auditor have accepted it.  This would be a great detail to get maybe even ILAC to come out with a position statement.  I am keeping the AB person who responded anonymous out of respect for their privacy.  But I believe the person is former PMEL and may even read this thread.  I wouldn't expect that person to be able to participate as an AB person.  But maybe the topic of derivative measurements should be brought up with ILAC (and/or other MRA(s)).
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: RFCAL on 10-16-2013 -- 16:19:50
listen to Scottbp---you cannot do as is stated. You cannot use ohm's law to get to a point and call that accredited. If your AB is telling you that you can, I would get another Ab's opinion. I would really get another AB. Do you want to tell us who the AB is? I would really like to know.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: John Treekiller on 10-16-2013 -- 20:58:25
Quote from: RFCAL on 10-16-2013 -- 16:19:50
listen to Scottbp---you cannot do as is stated. You cannot use ohm's law to get to a point and call that accredited. If your AB is telling you that you can, I would get another Ab's opinion. I would really get another AB. Do you want to tell us who the AB is? I would really like to know.
I've been following this from the start.  I guess it's time to throw my two cents in.  Every reply talks about larger resistances and the scope covered, and a few people have responded that you can't exceed the scope using Ohm's Law.  Just to ask a question; how do you go about calibrating a current shunt without using Ohm's Law?  Very few Meters measure resistances accurately below 0.1 Ohms, there are too many floor adders.  You apply an amount of current, measure the voltage and calculate the actual resistance versus the specified.  I would think that's a certifiable parameter and I would imagine that there are people that are accredited to calibrate current shunts.  I would believe that doing the same thing for larger resistances SHOULD be accredited, but I'm not an AD so I do not make those judgments, but it would be a way I would explain to an AD why I performed a measurement using that method.  Hope this helps, just an old retired tech's opinion.
Title: Re: An ISO17025 Question About Derivative Measurements from CMC
Post by: USMC kalibrater on 10-17-2013 -- 04:47:40
Quote from: RFCAL on 10-16-2013 -- 16:19:50
listen to Scottbp---you cannot do as is stated. You cannot use ohm's law to get to a point and call that accredited. If your AB is telling you that you can, I would get another Ab's opinion. I would really get another AB. Do you want to tell us who the AB is? I would really like to know.

You are correct in the fact that I just cannot just report a result in ohms, call it accredited but that is not what we are saying. 
What we are saying is to use your accredited current source, measure and your voltage measure capabilities to setup a measurement.  You apply a current and measure the voltage drop across a resistor.  We measure and report both on the report of calibration.   Then we mathmatically extrapolate the unit ohms and report the correct uncertainty on the report of calibration.  The accredited measurements voltage, current and a derived unit in ohms is supplied to the customer. 

Additionally their AB added that I cannot use this method and report a tighter uncertainty than is already listed on their CMC.   In other words if I reported .1% +/- x  for some values as my uncertainty on my scope I cannot list any uncertainty better than this even if the uncertainty would be better using the alternative method.  Its kind of a "duh" statement in my opinion.